IchiBan’s Citrus Peel Extraction and Pain Relief Topical

By Troy Ivan
ibc@ichibancrafter.com

I’ve been experimenting with citrus peel extraction for joint pain and inflammation for a few years and I’m so excited for the relief it’s brought so many people.  It’s my pleasure to share this with everyone who would like to give it a try.  It’s very easy to make, very fast-acting, all-natural, and quite frankly, too good to be true.  The first time that I really woke up to what I had was when I tried it on my elderly mother, who was having trouble walking and really struggled to walk up the stairs to go to bed when visiting.  Her ankles were so painful she was nearly incapacitated, so she became my first volunteer.  I had a batch of orange and lemon peel extract I’d recently made and already combined with coconut oil to be used as a topical, so we put that on her pained ankles to see what would happen, and I went back downstairs.  After about 5 minutes, she was calling my name from upstairs, so I went up expecting that she was going to ask for ice, ibuprofen, or something else for the pain, but she was sitting on the bed with a confused look on her face and said, “You aren’t going to believe this, but the pain is gone.”  I made the stuff and put it on her ankle, hoping for the best, but even I thought it was too fast and effective to be believed.  We kept experimenting with it, and every time, without fail, it eradicated the arthritic pain in her ankle.  Most interesting was the cumulative effect it appeared to have.  In the beginning, she would apply the topical every day but soon realized she didn’t need it so often, so it became once a week, once every two weeks, and finally only periodically when the pain came back. She was so happy to be pain-free but still said, “If it wasn’t me using it and experiencing the results, I wouldn’t believe it.”  She had tried everything, and this was the only thing that helped, and it helped miraculously.  Since then, I’ve given it to many people and taught many how to make it, and it hasn’t failed yet.  My hope is sharing this discovery and how to make it will help you with joint pain and inflation troubles.

MAKING THE CITRUS PEEL CONCENTRATE

I use food-grade ethanol extraction to make the full spectrum of orange and lemon peel concentrated oils known as ‘absolute oils.’  To perform the extraction and recover the ethanol safely at low temperatures, I use the DIY Vacuum Still system I put together. If you are unfamiliar with the process of ethanol extraction, go to my main page, www.ichibancrafter.com, and check out some of the extraction how-to posts for some great knowledge.

For the concentrate, I use equal amounts of orange and lemon peels for the extraction, but I encourage you to experiment using just one of them or different ratios if you think it might work better for you.  Dried peels can either be purchased or prepared yourself.  It takes a lot more time and effort to prepare your own, but the color you get from the extraction is incredible compared to the oil you get from processed dried peel.  Ideally, peels used for extraction should include only the outermost skin, not including any pith, and be dried completely, preferably with a food dehydrator.  You can use cut or ground-up peels for your ethanol extraction. 

Left: Dried orange and lemon peels Right: Making the wash

Ground peels have proven to provide a higher yield of oil but provide two difficulties over diced peels that require attention.  First, a good filtration plan is necessary as the powdery material will be difficult to filter well.  To keep your final extraction clean and sediment free you will most likely need something like a Buchner funnel to do the job.  Second, while the peels are soaking in ethanol, they will settle in a compacted sediment layer, so you will have to remember to shake it up once in a while for the ethanol to circulate through the material.  Working with the material in a chopped form will result in less yield but require less effort to process. 

The extraction can be performed with the orange and lemon peels together or separately, either way works equally as well.  I crafted 120 ml of concentrate oil using 2 lbs. of purchased peel soaked for 2 days with periodic agitation.  You can use smaller amounts for smaller personal sized batches, a little of this oil goes a long way.  My first couple of runs used just a couple of ounces of peels and got plenty of oil for personal use formulation size.

13 ml of orange and lemon peel concentrate straight out of the source turbo by ExtractCraft

WINTERIZATION

Winterization is a simple process to eliminate lipids and wax from an ethanol extraction.  After soaking the peels in ethanol and filtering out the solids from the solution, we have the “wash” containing all components mentioned earlier, as well as lipids and wax.  The lipids and wax are not necessarily undesirable for topicals because we will normally add in some form into the final formulation.  The problem is they can be a little messy with the extraction, and if a really pure oil is preferred, removing the fats and lipids makes quite a bit of difference.  Once they are removed, they can be saved to incorporate later or used in another project. 

Left: Wash ready for freezer Right: Wash at frozen temp with lipids and wax chunks floating and a layer on the bottom

The concept is simple: when the wash is subjected to freezing temperatures, the lipids and fats coagulate and precipitate out of the solution in a semi-solid state, then you just rough filter to separate.  Here are the simple steps:

  1. Put a well-filtered wash in the freezer for 48 hours or with dry ice for 3 hours.
  2. Don’t touch it or move it while it sets up.
  3. Remove it from the cold and run it through a medium/fast flow filter around 12-25 microns. An unbleached coffee filter is around 20-25 microns and can work fine, but a Buchner funnel can be used for better filtration and ethanol recovery.
  4. The resulting wash is ready for the ethanol recovery stage of extraction, and the separated lipids and fats can be used as desired.
Buchner funnel filtered lipids and wax

RESIDUAL ETHANOL

With ethanol extraction, people often ask, “How do you know if all the ethanol is out of the oil?”  I get the feeling that most people ask this question without really understanding what the question actually means or what if any, problem is caused by minute amounts of residual ethanol.  The truth is there will always be some residual ethanol, but it’s food-grade and a very minor amount.  Then, once that very minute amount of residual ethanol in the oil is incorporated into the larger formulation volume it will be diluted even further, so I’m not concerned and add it directly into my mix.

INCORPORATING CONCENTRATE WITH FORMULATION

You can use complex formulations or something as simple as solid-form coconut oil alone. 

Citrus peel extract pain relief topical

WARNINGS AND CAUTIONS

Now that you know how to make the amazing citrus peel extraction for joint pain and inflammation, there are a few warnings and cautions to keep in mind:

  • Citrus peel concentrates are extremely strong and the components of the citrus peel concentrate can cause skin irritation, especially if used at full potency, so test just a small amount of your formulation before jumping in fully. 
  • Citrus peel extractions, with or without ethanol, are flammable, so they must be kept away from an ignition source.
  • The citrus peel extraction is very photosensitive and can cause sunburn if applied to the skin and exposed to sunlight. It is not recommended to use this kind of formulation on skin that will be outside in direct sunlight.
  • The pigments from the citrus peels contained in formulation can stain fabric so use caution with what it comes into contact with before it is fully absorbed.
  • I am not a medical professional, so before using any information in this post, you should consult your medical professional to make sure this type of product is safe for you to use.

I HOPE YOU ENJOY THIS GREAT PAIN RELIEVER. STAY LIFTED MY FRIENDS !!!!!

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26 thoughts on “IchiBan’s Citrus Peel Extraction and Pain Relief Topical

    1. I’ve never used them but I’m not aware of any reason you couldn’t use them.

  1. My first filtered liquid looked very clear (dark green). I used my Buchner filter and a combination 2.5 micron filter for a second filtration and it still looks awfully clear. Do I still need to winterize it? I am using it for a pain topical.

    1. You don’t really “need” to do anything, it’s more about what you prefer for what you are making. The wash will be mostly clear without winterizing, the lipids and waxes in a room temp wash will not be visible until freezing. Having said all of that, for topicals I’d say winterizing isn’t really necessary.

  2. I am half way in, orange done and lemon with a day to go. Then I will extract each with my Source. Normally I add 2-4 gm of cannabinoid oil to four ounces of base cream to make topical salve. (Good Earth Soap’s Garden Balm is perfect for this). Do you have any suggestions as to how many grams of the citrus oil should be combined with the 120 gram base?

    It is inexpensive to make, and I want a potent cream, but don’t want to be wasteful. Thanks in advance.

    1. Based on your formula if my math is right, your recipe is 15% citrus oil (120/800 =15% x my 120 would be 18 gm).

      1. Kirby Mitlon: how do you combine the concentrate with the Garden Balm — do you simply stir in or do you use some heat?

    2. I use pretty much the weighting in my article. Its a personal preference and a personal tolerance consideration. Everyone is different

      1. Is it 120 ml or 120 grams that you stated you incorporated ? Earlier on in the article it says you extracted 120 ml from 2 lbs and then under the incorporation heading it states you extracted 120 grams. In general how much would one add of citrus oil in a recipe in terms of ml per oz or grams per oz ? Very interested in trying this out !

      2. 1g is pretty close to the same as 1ml so I may use them interchangeably. Probably should be consistent but I may not have been

    1. Depends on the material. The semi ground up stuff can be just 2-3 days. Larger chunks I do about a week or so

  3. Hello and thank you or this information!

    I have a Source but I also have some 100% lemon oil and 100% orange oil from LorAnns Oils in dram sizes: one lemon and one orange will be 7mL+. I also have organic coconut oil on hand. With 15% combined oils, I think I should mix the 7+ mL of citrus oils to 45g of melted coconut oil and 1g lecithin (2% of compound).

    Do those portions sound right?

    Thank you!

    John Geary

    1. I’m not sure, I haven’t used those oils and am not sure how they would work or what proportion to recommend.

    2. You can make 120 grams of pure oil for around $50. Buying lorann oil is way more expensive and it is not organic.

  4. Wondering if using dmso added would help absorption or if the lemon and orange is too strong and would cause burning.

  5. Just started to make this and am loving it on my arthritic thumb! Question for you, what is lost if you mix everything while warm? It’s so much easier to mix and then pour it into containers vs doing it while balm has started hardening. Also it’s hard to get the wax to combine with the rest of the ingredients without getting it hot enough to melt?

    1. And I should mention it is not separating because I keep mixing it until just before it’s no longer pourable and then I pour it into the containers. Haven’t had separation so far.

      1. If you don’t have separation then it shouldn’t be any problem at all. I hope it continues to help!

    2. A little warm should do the trick. The problem as mentioned in the post is you may end up with separation and the higher water components falling out

    3. I just had the same issue and found that as things cool down with a spatula I was able to mix it into the base. Really powerful salve!!

  6. Hello, and thanks for posting this. Are there any updates about lethicin? I assume one would use liquid sunflower lethicin, but I would be interested in anyones ideas about amounts and where in the process it would be incorporated. My experience with that stuff is that it is very hard to mix well, and is the stickiest mess imaginable to clean up!

  7. For a proof of concept, could one make an equivalent using essential oils from the health food store? I have two arthritic relatives, so a 50g pot of balm each would make a good present and tester size to see if this active ingredient works for them. I am familiar with making my own skin balms, but don’t have any experience or equipment for doing my own extractions.

    1. Not really. Essential oils aren’t as strong as absolutes. They might work to some extent

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